Distillation of ethylene glycol and antifreeze, explanation

We often receive inquiries for distillation of antifreeze.  Antifreeze can be distilled, but it is important to know what your objective is when trying to reclaim or concentrate antifreeze.

Antifreeze can be either Ethylene Glycol or Diethylene  Glycol, each of which has different properties that must be considered.  Ethylene Glycol has a boiling point of 135C and Diethylene Glycol has a boiling point of 240-250C.  The water in which it is mixed has a boiling point of 100C.

The first point to be considered is whether you are going to condense or concentrate your antifreeze, or actually distill the antifreeze.  

To condense the antifreeze is simply to distil the water contained in the antifreeze, thus removing the water and leaving the antifreeze behind in the distillation chamber.  When you do this the water is removed and everything else remains behind.  Water can be remixed to control the percentage of antifreeze in the solution to be reused.

If you want to distill the antifreeze and obtain a purity of the glycol, you must apply the options for solvent separation.  Utilizing separation, you would first remove the water from the waste antifreeze.  In a second cycle (automatically), you would distill the glycol at a higher temperature and remove the glycol from the waste antifreeze.  This will leave the additives, dirt, debris, and oils behind in the distillation chamber.

To distill Ethylene Glycol, a standard distillation unit is sufficient.  

For distillation of Diethylene Glycol, you need to use the vacuum option to reduce the boiling point of the Glycol.

In any case when removing water, it is required to apply option "G", which doubles the amount of heating capacity in the distillation unit.


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Last modified: March, 2010 05:05:00 AM